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Fifth Lab Task: Testing of adhesives on sea floor volcanic rocks collected by Alvin

volcanic rocks collected on Alvin mission to ocean floor

We have identified two epoxies that stick to rocks when applied underwater. They are "Smart Glue" and Ace hardware store #10232 water-proof epoxy putty. When sold in bulk, Smart Glue is named PSI-326 (Polymeric Systems). Use it in small amounts. The reaction is exothermic! Use the fume hood.

Today's goals:

  • Verify that the two adhesives will stick to volcanic rock when applied underwater.
  • Test adhesives in ice water to be sure that they will cure under cold conditions.

Send out one group to collect three buckets of seawater. Send out another group to collect a bucket of ice cubes from the mess. Chill some seawater. You may add the ice to the water, which will lower the salinity. You could also set a container of seawater onto a bed of ice to cool the seawater without diluting it.

Smart Glue

  1. Glue a piece of glass to the volcanic rock under seawater.
  2. Glue a piece of metal to the volcanic rock under seawater.
  3. Mix up a batch of Smart Glue with glitter. Attempt to write "MMA" on one of the rocks under seawater, using a wooden stick as a brush.
  4. Glue glass or metal to a volcanic rock in chilled seawater. Measure the temperature of the water. Observe whether the cure time is longer in cold water.
  5. After you have recorded all your observations, put all the samples in one covered tray and store in laboratory at room temperature until Thursday when we will show them to Dr. Tivey.

Ace water-proof epoxy putty

  1. Glue a piece of glass to the volcanic rock under seawater.
  2. Glue a piece of metal to the volcanic rock under seawater.
  3. Glue glass or metal to a volcanic rock in chilled seawater. Measure the temperature of the water. Observe whether the cure time is longer in cold water.
  4. After you have recorded all your observations, put all the samples in another covered tray and store in laboratory at room temperature until Thursday when we will show them to Dr. Tivey.

Shown below are the lab benches with trays holding seawater. Also shown are the volcanic rocks, with various attachments bonded with PSI-326 and Ace water proof epoxy putty. The samples have been prepared in seawater and stored in seawater for 48 hours before they were removed to examine the bonds. Glitter powder was added to the transparent PSI-326. Tabs of plastic and glass slides and roofing nails can be seen attached to the rocks.